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Weight:70g
(2E)-3-(1 ,3-benzodioxol-5-yl)-2-propenoyl chloride: To 2500 ml of toluene, placed in a 6 L reactor equipped with mechanical stirrer and thermometer, 500 g of (2E)-3-(1 ,3-benzodioxol-5-yl)-2-propenoic acid (2.6 mol, 1 eq.) is added, followed by 379.6 ml of SOCI2 (5.2 mol, 2 eq.) and 0.5 ml of DMF (no exotherm)
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