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The mixture was added to TBA/NaOH, vortexed and heated in a boiling water bath (100°C) for 30 min

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( 10.1093/chemse/18.6.661) [DOI] [Google Scholar] 56.Noe F, Polster J, Geithe C, Kotthoff M, Schieberle P, Krautwurst D